2,5-Di­methylhexane-2,5-diol at 110 K

R. B. Helmholdt; H. Reynaers

doi:10.1107/S0567740876007498

2,5-Dimethylhexane-2,5-diol at 110 K

R. B. Helmholdt, H. Reynaers

Faculty of Science and Engineering

Research output: Contribution to journal › Comment/Letter to the editor › Academic › peer-review

Abstract

CSH1802, monoclinic, P2~/c; a= 15.590 (3), b=9.948 (4), c=8.932 (2) A, fl=91.80 (2) ° at ll0K; Z=6, Do(293K)=l.0, Dc(l10K)=l.045 g cm-3; /z(Mo)=0.79 cm -t. The structure was solved by the symbolic addition method. Least-squares refinement gave R=0.085 and Rw=0.116 for 4057 observed reflexions (I>33). Hydrogen bonds connect the molecules into zigzag layers parallel to (100).

Original language	English
Pages (from-to)	2243-2245
Number of pages	3
Journal	Acta Crystallographica Section B: Structural Science
Volume	32
DOIs	https://doi.org/10.1107/S0567740876007498
Publication status	Published - Jul-1976

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@article{a91550dd24624492b00c73c403ccde0a,

title = "2,5-Dimethylhexane-2,5-diol at 110 K",

abstract = "CSH1802, monoclinic, P2~/c; a= 15.590 (3), b=9.948 (4), c=8.932 (2) A, fl=91.80 (2) ° at ll0K; Z=6, Do(293K)=l.0, Dc(l10K)=l.045 g cm-3; /z(Mo)=0.79 cm -t. The structure was solved by the symbolic addition method. Least-squares refinement gave R=0.085 and Rw=0.116 for 4057 observed reflexions (I>33). Hydrogen bonds connect the molecules into zigzag layers parallel to (100). ",

author = "Helmholdt, {R. B.} and H. Reynaers",

year = "1976",

month = jul,

doi = "10.1107/S0567740876007498",

language = "English",

volume = "32",

pages = "2243--2245",

journal = "Acta Crystallographica Section B: Structural Science",

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TY - JOUR

T1 - 2,5-Dimethylhexane-2,5-diol at 110 K

AU - Helmholdt, R. B.

AU - Reynaers, H.

PY - 1976/7

Y1 - 1976/7

N2 - CSH1802, monoclinic, P2~/c; a= 15.590 (3), b=9.948 (4), c=8.932 (2) A, fl=91.80 (2) ° at ll0K; Z=6, Do(293K)=l.0, Dc(l10K)=l.045 g cm-3; /z(Mo)=0.79 cm -t. The structure was solved by the symbolic addition method. Least-squares refinement gave R=0.085 and Rw=0.116 for 4057 observed reflexions (I>33). Hydrogen bonds connect the molecules into zigzag layers parallel to (100).

AB - CSH1802, monoclinic, P2~/c; a= 15.590 (3), b=9.948 (4), c=8.932 (2) A, fl=91.80 (2) ° at ll0K; Z=6, Do(293K)=l.0, Dc(l10K)=l.045 g cm-3; /z(Mo)=0.79 cm -t. The structure was solved by the symbolic addition method. Least-squares refinement gave R=0.085 and Rw=0.116 for 4057 observed reflexions (I>33). Hydrogen bonds connect the molecules into zigzag layers parallel to (100).

U2 - 10.1107/S0567740876007498

DO - 10.1107/S0567740876007498

M3 - Comment/Letter to the editor

SN - 0108-7681

VL - 32

SP - 2243

EP - 2245

JO - Acta Crystallographica Section B: Structural Science

JF - Acta Crystallographica Section B: Structural Science

ER -